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Beilstein J. Org. Chem. 2017, 13, 762–767, doi:10.3762/bjoc.13.75
Graphical Abstract
Scheme 1: Desymmetrization of cyclohexadienone by tethered nucleophile.
Scheme 2: Scope of the transformation.
Figure 1: Chiral iminophosphorane catalysts surveyed.
Scheme 3: Convex facial additions.
Scheme 4: Attempted oxidative deacylation.
Scheme 5: Attempted desulfurization with Raney nickel.
Beilstein J. Org. Chem. 2013, 9, 166–172, doi:10.3762/bjoc.9.19
Scheme 1: (A) Silyl glyoxylates as versatile reagents for three-component coupling reactions: representative ...
Scheme 2: Potential applications of silyl glyoxylate couplings and precedent synthetic intermediates toward t...
Scheme 3: Three-component coupling with a vinyl nucleophile and elaboration to Ichihara’s aldehyde.
Scheme 4: Modified Julia olefination as a step-efficient alternative endgame strategy.
Scheme 5: Three-component coupling with an allyl nucleophile and demonstration of successful ruthenium-cataly...
Scheme 6: Approaches considered to address the stereochemical issue.
Scheme 7: Use of a dithiane moiety to excert stereochemical control in the three-component coupling reaction ...
Scheme 8: Synthesis of a vinyl iodide for nucleophile generation and its use in a three-component coupling re...